{"id":150,"date":"2017-12-04T15:53:26","date_gmt":"2017-12-04T06:53:26","guid":{"rendered":"http:\/\/133.38.206.236\/HP\/?page_id=150"},"modified":"2017-12-04T15:55:42","modified_gmt":"2017-12-04T06:55:42","slug":"tlc%e7%94%a8%e7%99%ba%e8%89%b2%e6%b6%b2%e3%81%ae%e8%aa%bf%e8%a3%bd%e6%b3%95%e3%81%a8%e7%94%a8%e9%80%94","status":"publish","type":"page","link":"https:\/\/md.fms.saitama-u.ac.jp\/?page_id=150","title":{"rendered":"TLC\u7528\u767a\u8272\u6db2\u306e\u8abf\u88fd\u6cd5\u3068\u7528\u9014"},"content":{"rendered":"<p><center><span style=\"color: #3333ff;\"><span style=\"font-size: medium;\">TLC\u7528\u767a\u8272\u6db2\u306e\u8abf\u88fd\u6cd5\u3068\u7528\u9014<\/span><\/span><\/center><\/p>\n<table border=\"\" width=\"93%\" bgcolor=\"#FFFFCC\">\n<tbody>\n<tr bgcolor=\"#DADBFE\">\n<td bgcolor=\"#DADBFE\"><center><span style=\"font-size: xx-small;\">\u691c\u51fa\u5bfe\u8c61<\/span><\/center><\/td>\n<td bgcolor=\"#DADBFE\"><center><span style=\"font-size: xx-small;\">\u691c\u51fa\u8a66\u85ac<\/span><\/center><\/td>\n<td align=\"CENTER\" bgcolor=\"#DADBFE\"><span style=\"font-size: xx-small;\">\u8a66\u85ac\u8abf\u88fd\u6cd5<\/span><\/td>\n<td bgcolor=\"#DADBFE\"><center><span style=\"font-size: xx-small;\">\u767a\u8272\u6cd5<\/span><\/center><\/td>\n<\/tr>\n<tr>\n<td bgcolor=\"#99FF99\">\u6709\u6a5f\u5316\u5408\u7269\u4e00\u822c<\/td>\n<td bgcolor=\"#99FF99\">\u30a2\u30cb\u30b9\u2015\u786b\u9178<br \/>\n(p-Anisaldehyde?Sulfuric acid?Methanol)<\/td>\n<td bgcolor=\"#99FF99\">p-\u30a2\u30cb\u30b9\u30a2\u30eb\u30c7\u30d2\u30c9(10 mL)\u3092\u30e1\u30bf\u30ce\u30fc\u30eb(85 mL)\u306b\u6eb6\u89e3\u3055\u305b\u3001\u6c37\u51b7\u4e0b\u3001\u6fc3\u786b\u9178(5 mL)\u3092\u3086\u3063\u304f\u308a\u6ef4\u4e0b\u3059\u308b\u3053\u3068\u306b\u3088\u308a\u8abf\u88fd\u3059\u308b\u3002\u8abf\u88fd\u3057\u305f\u6eb6\u6db2\u306f\u3001\u51b7\u6697\u6240\u306b\u3066\u4fdd\u5b58\u306e\u3053\u3068\u3002<\/td>\n<td bgcolor=\"#99FF99\">\u5c55\u958b\u6e08\u307f\u306eTLC\u7248\u306b\u3001\u5674\u9727\u3042\u308b\u3044\u306f\u30c7\u30a3\u30c3\u30d7\u65b9\u5f0f\u306b\u3088\u308a\u8abf\u88fd\u3057\u305f\u6eb6\u6db2\u3092\u5857\u5e03\u3059\u308b\u3002\u305d\u306e\u5f8c\u3001\u30db\u30c3\u30c8\u30d7\u30ec\u30fc\u30c8\u4e0a\u306b\u304a\u3044\u3066\u3001\u71b1\u3092\u304b\u3051\u308b\u3002\u6709\u6a5f\u7269\u306e\u30b9\u30dd\u30c3\u30c8\u304c\u7126\u3052\u3066\u304f\u308b\u3002\u80cc\u666f\u306f\u7d2b\u8272\u304b\u3089\u8d64\u7d2b\u8272\u306b\u306a\u308a\u3001\u5316\u5408\u7269\u306b\u3088\u3063\u3066\u3001\u7a2e\u3005\u306e\u8272\u3092\u5448\u3059\u308b\u3053\u3068\u304c\u3042\u308b\u3002<\/td>\n<\/tr>\n<tr>\n<td bgcolor=\"#99FF99\"><\/td>\n<td bgcolor=\"#99FF99\">\u30ea\u30f3\u30e2\u30ea\u30d6\u30c7\u30f3\u9178<br \/>\n(5% Ethanolic Phosphomolybdic acid)<\/td>\n<td bgcolor=\"#99FF99\">\u30ea\u30f3\u30e2\u30ea\u30d6\u30c7\u30f3\u9178(12MoO<sub>3<\/sub>\uff65H<sub>3<\/sub>PO<sub>4<\/sub>\uff65xH<sub>2<\/sub>O)\u3092\u30a8\u30bf\u30ce\u30fc\u30eb\u306b\u6eb6\u89e3\u3055\u305b\u3001\u7d045%\u306e\u6fc3\u5ea6\u306b\u8abf\u88fd\u3059\u308b\u3002<\/td>\n<td bgcolor=\"#99FF99\">\u00a0\u5c55\u958b\u6e08\u307f\u306eTLC\u7248\u306b\u3001\u5674\u9727\u3042\u308b\u3044\u306f\u30c7\u30a3\u30c3\u30d7\u65b9\u5f0f\u306b\u3088\u308a\u8abf\u88fd\u3057\u305f\u6eb6\u6db2\u3092\u5857\u5e03\u3059\u308b\u3002\u305d\u306e\u5f8c\u3001\u30db\u30c3\u30c8\u30d7\u30ec\u30fc\u30c8\u4e0a\u306b\u304a\u3044\u3066\u3001\u71b1\u3092\u304b\u3051\u308b\u3002\u6709\u6a5f\u7269\u306e\u30b9\u30dd\u30c3\u30c8\u304c\u7126\u3052\u3066\u304f\u308b\u3002\u80cc\u666f\u306f\u6df1\u7dd1\u8272\u306b\u306a\u308b\u3002<\/td>\n<\/tr>\n<tr>\n<td bgcolor=\"#99FF99\"><\/td>\n<td bgcolor=\"#99FF99\">\u30e8\u30a6\u7d20<br \/>\n(Iodine vapor)<\/td>\n<td bgcolor=\"#99FF99\"><\/td>\n<td bgcolor=\"#99FF99\">\u30e8\u30a6\u7d20\u84b8\u6c17\u4e0b\u306b\u8584\u5c64\u677f\u3092\u7f6e\u304f\u3068\u3001\u6709\u6a5f\u5316\u5408\u7269\u306e\u30b9\u30dd\u30c3\u30c8\u90e8\u5206\u306b\u8d64\u304b\u3089\u8336\u306e\u5448\u8272\u304c\u8d77\u304d\u308b\u3002\u306a\u304a\u3001\u53d6\u308a\u51fa\u3059\u3068\u3001\u767a\u8272\u304c\u6d88\u3048\u308b\u306e\u3067\u3001\u76f4\u3050\u306b\u30b9\u30dd\u30c3\u30c8\u3092\u30de\u30fc\u30af\u3059\u308b\u3053\u3068\u3002\u307e\u305f\u3001\u84b8\u6c17\u306e\u5438\u5165\u306f\u6975\u529b\u907f\u3051\u308b\u3053\u3068\u3002<\/td>\n<\/tr>\n<tr>\n<td bgcolor=\"#FFCCCC\">\u30a2\u30df\u30ce\u57fa<\/td>\n<td bgcolor=\"#FFCCCC\">\u30cb\u30f3\u30d2\u30c9\u30ea\u30f3\u6eb6\u6db2<br \/>\n(Ninhydrin)<\/td>\n<td bgcolor=\"#FFCCCC\">\u30cb\u30f3\u30d2\u30c9\u30ea\u30f3\u3092\u30a8\u30bf\u30ce\u30fc\u30eb\u306b\u6eb6\u89e3\u3055\u305b\u30010.7%\u306e\u6fc3\u5ea6\u306b\u8abf\u88fd\u3059\u308b\u3002<\/td>\n<td bgcolor=\"#FFCCCC\">\u5674\u9727\u5f8c\u3001\u30db\u30c3\u30c8\u30d7\u30ec\u30fc\u30c8\u4e0a\u3067\u52a0\u71b1\u3059\u308b\u3068\u3001\u30a2\u30df\u30ce\u57fa\u3092\u542b\u3093\u3067\u3044\u308b\u30b9\u30dd\u30c3\u30c8\u90e8\u5206\u306b\u8d64\u304b\u3089\u7d2b\u8272\u306e\u767a\u8272\u304c\u8d77\u304d\u308b\u3002<\/td>\n<\/tr>\n<tr>\n<td bgcolor=\"#FFCC99\">\u4e8c\u91cd\u7d50\u5408<\/td>\n<td bgcolor=\"#FFCC99\">\u30ab\u30e1\u30ec\u30aa\u30f3\u6eb6\u6db2<br \/>\n(5 wt% aq. Potassium permanganate)<\/td>\n<td bgcolor=\"#FFCC99\">\u904e\u30de\u30f3\u30ac\u30f3\u9178\u30ab\u30ea\u30a6\u30e0(KMnO<sub>4<\/sub>)\u3092\u84b8\u7559\u6c34\u306b\u6eb6\u89e3\u3055\u305b\u30015 wt%\u306e\u6fc3\u5ea6\u306b\u8abf\u88fd\u3059\u308b\u3002<\/td>\n<td bgcolor=\"#FFCC99\">\u5674\u9727\u5f8c\u3001\u4e8c\u91cd\u7d50\u5408\u3092\u542b\u3093\u3067\u3044\u308b\u30b9\u30dd\u30c3\u30c8\u304c\u9ec4\u8272\u306b\u5448\u8272\u3059\u308b\u3002\u30d0\u30c3\u30af\u306f\u3001\u6fc3\u3044\u7d2b\u8272\u306a\u306e\u3067\u3001\u591a\u5c11\u898b\u306b\u304f\u3044\u3053\u3068\u304c\u3042\u308b\u3002\u307e\u305f\u3001\u30db\u30c3\u30c8\u30d7\u30ec\u30fc\u30c8\u4e0a\u3067\u52a0\u71b1\u3059\u308b\u3068\u3001\u3088\u308a\u5448\u8272\u3059\u308b\u5834\u5408\u3082\u3042\u308b\u3002<\/td>\n<\/tr>\n<tr>\n<td>\u30b1\u30c8\u30f3\u30fb\u30a2\u30eb\u30c7\u30d2\u30c9<\/td>\n<td>DNPH\u6eb6\u6db2<br \/>\n(2,4-Dinitrophenylhydrazine)<\/td>\n<td>DNPH (0.4 g)\u30922M-HCl(100 mL)\u3068\u30a8\u30bf\u30ce\u30fc\u30eb(100 mL)\u306e\u6df7\u5408\u6eb6\u5a92\u306b\u6eb6\u89e3\u3055\u305b\u3001\u8abf\u88fd\u3059\u308b\u3002<\/td>\n<td>\u5674\u9727\u5f8c\u3001\u30ab\u30eb\u30dc\u30cb\u30eb\u57fa\u3092\u542b\u3093\u3067\u3044\u308b\u30b9\u30dd\u30c3\u30c8\u304c\u9ec4\u8272\u306b\u5448\u8272\u3059\u308b\u3002\u307e\u305f\u3001\u30db\u30c3\u30c8\u30d7\u30ec\u30fc\u30c8\u4e0a\u3067\u52a0\u71b1\u3059\u308b\u3068\u3001\u30b1\u30bf\u30fc\u30eb\u3084\u30a2\u30bb\u30bf\u30fc\u30eb\u3082\u767a\u8272\u3059\u308b\u3002<\/td>\n<\/tr>\n<tr bgcolor=\"#FFCCFF\">\n<td>\u30ab\u30eb\u30dc\u30ad\u30b7\u30eb\u57fa<\/td>\n<td>\u30d6\u30ed\u30e2\u30af\u30ec\u30be\u30fc\u30eb\u30b0\u30ea\u30fc\u30f3\u6eb6\u6db2<br \/>\n(0.04 wt% aq. Bromocresol Green)<\/td>\n<td>3\u2019,3\u2019\u2019,5\u2019,5\u2019\u2019-tetrabrom-m-cresolsulfonephthalein\u3092\u84b8\u7559\u6c34\u306b\u6eb6\u89e3\u3055\u305b\u30010.04 wt%\u306e\u6fc3\u5ea6\u306b\u8abf\u88fd\u3059\u308b\u3002<\/td>\n<td>\u5674\u9727\u5f8c\u3001\u30ab\u30eb\u30dc\u30ad\u30b7\u30eb\u57fa\u3092\u542b\u3093\u3067\u3044\u308b\u30b9\u30dd\u30c3\u30c8\u304c\u9ec4\u8272\u306b\u5448\u8272\u3059\u308b\u3002\u904a\u96e2\u306e\u30ab\u30eb\u30dc\u30ad\u30b7\u30eb\u57fa\u304c\u304a\u3088\u305dpH 4\u3092\u793a\u3059\u3053\u3068\u306b\u57fa\u3065\u304f\u5909\u8272\u3067\u3042\u308b\u3002<\/td>\n<\/tr>\n<tr bgcolor=\"#E8FFDD\">\n<td>\u5171\u5f79\u7cfb\u5316\u5408\u7269<\/td>\n<td>UV\u30e9\u30f3\u30d7<\/td>\n<td><\/td>\n<td>\u5171\u5f79\u7cfb\u306e\u5b58\u5728\u3059\u308b\u5316\u5408\u7269\u306e\u53ef\u8996\u5316\u306b\u5229\u7528\u3059\u308b\u3002\u7279\u306b\u3001<i><span style=\"font-family: Symbol;\">a<\/span><\/i>,<i><span style=\"font-family: Symbol;\">b<\/span><\/i>-\u4e0d\u98fd\u548c\u30b1\u30c8\u30f3\u3084\u30d9\u30f3\u30bc\u30f3\u74b0\u3092\u542b\u3080\u5316\u5408\u7269\u306e\u691c\u51fa\u306b\u306f\u6709\u52b9\u3067\u3042\u308b\u3002<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<p>&nbsp;<\/p>\n","protected":false},"excerpt":{"rendered":"<p>TLC\u7528\u767a\u8272\u6db2\u306e\u8abf\u88fd\u6cd5\u3068\u7528\u9014 \u691c\u51fa\u5bfe\u8c61 \u691c\u51fa\u8a66\u85ac \u8a66\u85ac\u8abf\u88fd\u6cd5 \u767a\u8272\u6cd5 \u6709\u6a5f\u5316\u5408\u7269\u4e00\u822c \u30a2\u30cb\u30b9\u2015\u786b\u9178 (p-Anisaldehyde?Sulfuric acid?Methanol) p-\u30a2\u30cb\u30b9\u30a2\u30eb\u30c7\u30d2\u30c9(10 mL)\u3092\u30e1\u30bf &#8230;<\/p>\n","protected":false},"author":1,"featured_media":0,"parent":7,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"footnotes":""},"class_list":["post-150","page","type-page","status-publish","hentry"],"_links":{"self":[{"href":"https:\/\/md.fms.saitama-u.ac.jp\/index.php?rest_route=\/wp\/v2\/pages\/150","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/md.fms.saitama-u.ac.jp\/index.php?rest_route=\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/md.fms.saitama-u.ac.jp\/index.php?rest_route=\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/md.fms.saitama-u.ac.jp\/index.php?rest_route=\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/md.fms.saitama-u.ac.jp\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=150"}],"version-history":[{"count":2,"href":"https:\/\/md.fms.saitama-u.ac.jp\/index.php?rest_route=\/wp\/v2\/pages\/150\/revisions"}],"predecessor-version":[{"id":154,"href":"https:\/\/md.fms.saitama-u.ac.jp\/index.php?rest_route=\/wp\/v2\/pages\/150\/revisions\/154"}],"up":[{"embeddable":true,"href":"https:\/\/md.fms.saitama-u.ac.jp\/index.php?rest_route=\/wp\/v2\/pages\/7"}],"wp:attachment":[{"href":"https:\/\/md.fms.saitama-u.ac.jp\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=150"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}